ABSTRACT
<p><b>OBJECTIVE</b>To study the chemical constituents of the stem and leaves from Curcuma wenyujin.</p><p><b>METHOD</b>The compounds were isolated by silica gel column chromatography in associating with Sephadex LH -20 chromatography. While their structures were identified on the basis of spectroscopic date.</p><p><b>RESULT</b>Nine sesquiterpenes were isolated and identified. Their structures were identified as curdione (1), neocurdione (2), trans, trans-germacrone (3), cis, trans-germacrone (4), curcumenone (5), curcumadione (6), isoprocurcumenol (7), glechomanolide (8) and (1R, 10R)-( -)-1, 10-dihydrocurdione (9).</p><p><b>CONCLUSION</b>All of these compounds were isolated from the stems and leaves of this plant for the first time.</p>
Subject(s)
Chromatography , Curcuma , Chemistry , Drugs, Chinese Herbal , Chemistry , Magnetic Resonance Spectroscopy , Plant Leaves , Chemistry , Plant Stems , Chemistry , SesquiterpenesABSTRACT
<p><b>AIM</b>To investigate the secondary metabolites of the mangrove plant Ceriops tagal.</p><p><b>METHODS</b>Column chromatography techniques including HPLC were used for the separation and purification, and extensive spectral analysis including various 2D NMR spectra were employed for structure elucidation.</p><p><b>RESULTS</b>Nine compounds, namely, tagalsins A (1), ent-5alpha-dolabr-4 (18) -ene-15S,16-diol (2), squalene (3), betulinic acid (4), lup-20 (29) -en-3-on-28-oic acid (5), betulin (6), lup-20 (29) -en-3-on-28-ol (7), beta-sitosterol (8), n-hexacosanylferulate (9) were obtained. Of which 1 and 2 belong to dolabrane diterpene.</p><p><b>CONCLUSION</b>Compound 1 is a new compound, and 2 to 9 are isolated from this species for the first time.</p>